GOLM METABOLOME DATABASE
How would you rate the quality of this mass spectrum?
poor, not helpful 
 outstanding, most helpful.
This spectrum was 0 times rated; on average=0.0

Erythronic acid-1,4-lactone (2TMS)

 

Replica Mass Spectra of Erythronic acid-1,4-lactone (2TMS)

replicalib entry datedetectionmethodspecies
805 June 2013  MRI_2013 
126 November 2004  M[FAME4090]Standard
212 May 2005  M[NIST] 
319 July 2007 MS-TOFVAR5Reference Substance
401 September 2001 MS-QuadM[2]Standard Addition
512 May 2005  M[NIST] 
701 December 2003 MS-QuadM[2]Standard Addition
7 spectrum(a)
rotate: click+drag; translate: alt+click+drag; zoom: mousewheel; save: mol

Spectrum Details

analyteErythronic acid-1,4-lactone (2TMS)
analyte InChIInChI=1S/C10H22O4Si2/c1-15(2,3)13-8-7-12-10(11)9(8)14-16(4,5)6/h8-9H,7H2,1-6H3/t8-,9-/m1/s1
analyte mass262.45
chromatogram6039hf_50
citation 
authorsBoelling C, Liebig F, Erban A, Kopka J, Max Planck Institute of Molecular Plant Physiology, Department of Molecular Plant Physiology (Prof. Willmitzer L), Am Muehlenberg 1, D-14476 Golm, Germany
lib entry date19 July 2007
metabolite roleMST
retention time (sec)449.64
retention index (VAR5 method, n-alkanes C10–C36) 
base peak (m/z)147
maximal intensity918.649
mass-intensity-peaks cardinality635 intensities
minimal m/z45
maximal m/z1.000
download JCAMP DXSpectrumJcampDx.ashx?id=01e40d5b-f407-4b36-ab5d-f490dfaefbe9
download MSPSpectrumMsp.ashx?id=01e40d5b-f407-4b36-ab5d-f490dfaefbe9

GC-Method

nameMDN35
citationKopka J, Max Planck Institute of Molecular Plant Physiology, Department of Molecular Plant Physiology (Prof. Willmitzer L), Am Muehlenberg 1, D-14476 Golm, Germany
attributetextdetails
deconvolutionChromaTOFBASELINE OFFSET: 1; SMOOTHING: 5; PEAK WIDTH: 3s; S/N: 10
derivatizationMEOX; MSTFAMETHOXYAMINATION: 120min at 37°C; TRIMETHYLSILYLATION: 30min at 37°C
detectorMS-TOFm/z = 70-600; scans:20/s;
extractionchloroform:dH2O (2:1; v/v); chloroform (20°C); dH2O (4°C)
ion sourceEI70eV
RIFAME, d6-CholesteroleFAME: C8, C9, C10, C12, C14, C16, C18, C20, C22, C24, C26, C28, C30
separationGCCOLUMN:35%phenyl-65%dimethylpolysiloxane, 30m, ID:0.32mm, DF:0.25µm, MDN-35 (Macherey-Nagel, Düren, Germany); PROGRAM:iso 2min 80°C, ramp 15°C/min, iso 6min 330°C; FLOW:Helium, 2mL/min; INJECTION:1µL, splitless, 230°C; TRANSFER:250°C; IONSOURCE:250°C

comments on this mass spectrum

Post a Comment
Name:
 
Website:  
Email:
Comments:
service last updated 17/02/2017 © 2008-2014 Golm Metabolome Database - All rights reserved
Top