How would you rate the quality of this mass spectrum?
poor, not helpful
outstanding, most helpful.
This spectrum was 0 times rated; on average=0.0
This png spectrum visualization works for backward compatibility reasons only, as
your browser does not support the HTML5
<canvas> element. To
enjoy zoom-in functionality please upgrade to a HTML5 ready Browser!
Replica Mass Spectra of Glucuronic acid (1MEOX) (5TMS) MP
| replica | lib entry date | detection | method | species |
| 2 | 22 February 2005 | MS-TOF | M[STR] | |
| 3 | 14 October 2003 | MS-Quad | M[2] | Standard |
| 15 | 28 August 2012 | | MassBank GC 2010 Tsujimoto | |
| 4 | 19 July 2007 | MS-TOF | VAR5 | Reference Substance |
| 5 | 01 May 2001 | MS-TOF | M[EIGTMS] | Solanum tuberosum |
| 6 | 22 February 2005 | MS-TOF | M[STR] | |
| 7 | 19 January 2005 | MS-QUAD | M[ROE] | |
| 9 | 12 October 2005 | MS-TRAP | M[BAR] | |
| 10 | 01 March 2002 | MS-Quad | M[2] | Standard |
| 11 | 15 March 2005 | MS-TOF | M[6] | Reference Substance |
| 15 spectrum(a) |
rotate: click+drag; translate: alt+click+drag;
zoom: mousewheel; save: mol
Spectrum Details
| analyte | Glucuronic acid (1MEOX) (5TMS) MP |
| analyte InChI | InChI=1S/C22H53NO7Si5/c1-25-23-17-18(26-31(2,3)4)19(27-32(5,6)7)20(28-33(8,9)10)21(29-34(11,12)13)22(24)30-35(14,15)16/h17-21H,1-16H3/b23-17+/t18-,19+,20-,21-/m0/s1 |
| analyte mass | 584.09 |
| chromatogram | NA(_43) |
| citation | |
| authors | Moritz T, Umea Plant Science Centre, Department of Forest Genetics and Plant Physiology, Swedish University of Agricultural Sciences, SE-901 83 Umea, Sweden |
| lib entry date | 25 January 2005 |
| metabolite role | METB |
| retention time (sec) | 338.1 |
| retention index (VAR5 method, n-alkanes C10–C36) | 1,923.47 (predicted, according to Strehmel, N. et.al) |
| base peak (m/z) | 73 |
| maximal intensity | 999 |
| mass-intensity-peaks cardinality | 188 intensities |
| minimal m/z | 53 |
| maximal m/z | 425 |
| download JCAMP DX | SpectrumJcampDx.ashx?id=1970ce8d-026c-4ee2-9c12-9341e2d6c5be |
| download MSP | SpectrumMsp.ashx?id=1970ce8d-026c-4ee2-9c12-9341e2d6c5be |
GC-Method
| name | M[MOR] |
| citation | Gullberg J, Jonsson P, Nordström A, Sjöström M, Moritz T (2004) Anal Biochem 331, 283-295 |
| attribute | text | details |
| deconvolution | ChromaTOF V1.00 (Pegasus Driver 1.61), LECO, St. Joseph, MI, USA | OFFSET:NA; SMOOTHING:NA; WIDTH:2; SN:>10 |
| derivatization | MEOX; TMS | METHOXYAMINATION: 60min60°C, 960min20°C; SILYLATION:>60min40°C |
| detector | MS-TOF | m/z:50-800; SCANS:30/s; Pegasus III TOF-MS; LECO, St. Joseph, MI, USA |
| extraction | methanol:chloroform:water (3:1:1; v/v/v) 15min at 60°C | |
| ion source | EI | 70eV |
| metabolic inactivation | cut; liquid nitrogen; -80°C | |
| partitioning | none | |
| RI | ALKANE | C12, C13, C14, C15, C16, C17, C18, C19, C20, C21, C22, C23, C24, C25 |
| separation | GC | COLUMN:5%diphenyl-95%dimethylpolysiloxane, 10m, ID:0.18mm, DF:0.18µm, DB-5-MS (J&W Scientific, Folsom, CA, USA); PROGRAM: iso 2min at 70°C, ramp 40°C/min, iso 1min at 320°C; FLOW:Helium, 1.0ml/min: INJECTION:1µL, splitless, 270°C; TRANSFER:250°C; IONSOURCE:200°C |
comments on this mass spectrum
Post a Comment
|
Name:
|
|
|
|
Website:
|
|
|
|
Email:
|
|
|
|
Comments:
|
|
|
|
|
|
