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Glucose, 1,6-anhydro-, beta- (3TMS)

 

Replica Mass Spectra of Glucose, 1,6-anhydro-, beta- (3TMS)

replicalib entry datedetectionmethodspecies
112 June 2003 MS-QuadM[2]Reference Substance
201 November 2001 MS-TOFM[EIGTMS]Corynebacterium glutamicum
312 May 2005  M[NIST] 
1507 January 2011 MS-TOFVAR5 
1410 December 2010 MS-TOFVAR5 
607 September 2004 MS-QuadM[2]Standard
701 May 2001 MS-TOFM[EIGTMS]Standard Addition
1828 August 2012  MassBank GC 2010 Tsujimoto 
1019 July 2007 MS-TOFVAR5Reference Substance
1905 June 2013  MRI_2013 
14 spectrum(a)
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Spectrum Details

analyteGlucose, 1,6-anhydro-, beta- (3TMS)
analyte InChIInChI=1S/C15H34O5Si3/c1-21(2,3)18-12-11-10-16-15(17-11)14(20-23(7,8)9)13(12)19-22(4,5)6/h11-15H,10H2,1-9H3/t11-,12-,13+,14-,15?/m1/s1
analyte mass378.68
chromatogram6058hf_55
citation 
authorsBoelling C, Liebig F, Erban A, Kopka J, Max Planck Institute of Molecular Plant Physiology, Department of Molecular Plant Physiology (Prof. Willmitzer L), Am Muehlenberg 1, D-14476 Golm, Germany
lib entry date19 July 2007
metabolite roleMETB
retention time (sec)543.84
retention index (VAR5 method, n-alkanes C10–C36) 
base peak (m/z)73
maximal intensity140,775
mass-intensity-peaks cardinality335 intensities
minimal m/z45
maximal m/z995
download JCAMP DXSpectrumJcampDx.ashx?id=19c462be-2e8a-4ea9-b5e8-4384afe89df3
download MSPSpectrumMsp.ashx?id=19c462be-2e8a-4ea9-b5e8-4384afe89df3

GC-Method

nameMDN35
citationKopka J, Max Planck Institute of Molecular Plant Physiology, Department of Molecular Plant Physiology (Prof. Willmitzer L), Am Muehlenberg 1, D-14476 Golm, Germany
attributetextdetails
deconvolutionChromaTOFBASELINE OFFSET: 1; SMOOTHING: 5; PEAK WIDTH: 3s; S/N: 10
derivatizationMEOX; MSTFAMETHOXYAMINATION: 120min at 37°C; TRIMETHYLSILYLATION: 30min at 37°C
detectorMS-TOFm/z = 70-600; scans:20/s;
extractionchloroform:dH2O (2:1; v/v); chloroform (20°C); dH2O (4°C)
ion sourceEI70eV
RIFAME, d6-CholesteroleFAME: C8, C9, C10, C12, C14, C16, C18, C20, C22, C24, C26, C28, C30
separationGCCOLUMN:35%phenyl-65%dimethylpolysiloxane, 30m, ID:0.32mm, DF:0.25µm, MDN-35 (Macherey-Nagel, Düren, Germany); PROGRAM:iso 2min 80°C, ramp 15°C/min, iso 6min 330°C; FLOW:Helium, 2mL/min; INJECTION:1µL, splitless, 230°C; TRANSFER:250°C; IONSOURCE:250°C

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