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Adenosine, alpha- (4TMS) MP

 

Replica Mass Spectra of Adenosine, alpha- (4TMS) MP

replicalib entry datedetectionmethodspecies
1628 August 2012  MassBank GC 2010 Ara 
101 November 2001 MS-TOFM[EIGTMS]Standard
612 October 2005 MS-TRAPM[BAR] 
1528 August 2012  MassBank GC 2010 Tsujimoto 
1428 August 2012  MassBank GC 2010 Kusano 
715 December 2003 MS-QuadM[2]Standard Addition
219 July 2007 MS-TOFVAR5Reference Substance
401 February 2005 MS-TOFM[6]Reference Substance
812 May 2005  M[NIST] 
901 May 2001 MS-TOFM[EIGTMS]Saccharomyces cerevisiae
15 spectrum(a)
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Spectrum Details

analyteAdenosine, alpha- (4TMS) MP
analyte InChIInChI=1S/C22H45N5O4Si4/c1-32(2,3)26-20-17-21(24-14-23-20)27(15-25-17)22-19(31-35(10,11)12)18(30-34(7,8)9)16(29-22)13-28-33(4,5)6/h14-16,18-19,22H,13H2,1-12H3,(H,23,24,26)/t16-,18-,19-,22+/m1/s1
analyte mass555.97
chromatogram6080hf_35
citation 
authorsBoelling C, Liebig F, Erban A, Kopka J, Max Planck Institute of Molecular Plant Physiology, Department of Molecular Plant Physiology (Prof. Willmitzer L), Am Muehlenberg 1, D-14476 Golm, Germany
lib entry date19 July 2007
metabolite roleMETB
retention time (sec)923.49
retention index (VAR5 method, n-alkanes C10–C36) 
base peak (m/z)73
maximal intensity954.263
mass-intensity-peaks cardinality693 intensities
minimal m/z45
maximal m/z1.000
download JCAMP DXSpectrumJcampDx.ashx?id=43679853-9844-4629-882f-63f148f53b1f
download MSPSpectrumMsp.ashx?id=43679853-9844-4629-882f-63f148f53b1f

GC-Method

nameMDN35
citationKopka J, Max Planck Institute of Molecular Plant Physiology, Department of Molecular Plant Physiology (Prof. Willmitzer L), Am Muehlenberg 1, D-14476 Golm, Germany
attributetextdetails
deconvolutionChromaTOFBASELINE OFFSET: 1; SMOOTHING: 5; PEAK WIDTH: 3s; S/N: 10
derivatizationMEOX; MSTFAMETHOXYAMINATION: 120min at 37°C; TRIMETHYLSILYLATION: 30min at 37°C
detectorMS-TOFm/z = 70-600; scans:20/s;
extractionchloroform:dH2O (2:1; v/v); chloroform (20°C); dH2O (4°C)
ion sourceEI70eV
RIFAME, d6-CholesteroleFAME: C8, C9, C10, C12, C14, C16, C18, C20, C22, C24, C26, C28, C30
separationGCCOLUMN:35%phenyl-65%dimethylpolysiloxane, 30m, ID:0.32mm, DF:0.25µm, MDN-35 (Macherey-Nagel, Düren, Germany); PROGRAM:iso 2min 80°C, ramp 15°C/min, iso 6min 330°C; FLOW:Helium, 2mL/min; INJECTION:1µL, splitless, 230°C; TRANSFER:250°C; IONSOURCE:250°C

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