GOLM METABOLOME DATABASE
How would you rate the quality of this mass spectrum?
poor, not helpful 
 outstanding, most helpful.
This spectrum was 0 times rated; on average=0.0

Xylulose (1MEOX) (4TMS) MP

 

Replica Mass Spectra of Xylulose (1MEOX) (4TMS) MP

replicalib entry datedetectionmethodspecies
1023 July 2012 MS-TOFVAR5 
810 December 2010 MS-TOFVAR5 
122 February 2005 MS-TOFM[STR] 
903 November 2010  Schomburg_GC_2010 
319 July 2007 MS-TOFVAR5Reference Substance
1228 August 2012  MassBank GC 2010 Kusano 
419 July 2007 MS-TOFMDN35Reference Substance
522 February 2005 MS-TOFM[STR] 
1528 August 2012  MassBank GC 2010 Ara 
1628 August 2012  MassBank GC 2010 Ara 
11 spectrum(a)
rotate: click+drag; translate: alt+click+drag; zoom: mousewheel; save: mol

Spectrum Details

analyteXylulose (1MEOX) (4TMS) MP
analyte InChIInChI=1S/C18H45NO5Si4/c1-20-19-16(14-21-25(2,3)4)18(24-28(11,12)13)17(23-27(8,9)10)15-22-26(5,6)7/h17-18H,14-15H2,1-13H3/b19-16+/t17-,18-/m1/s1
analyte mass467.9
chromatogramNA(_43)
citation 
authorsMoritz T, Umea Plant Science Centre, Department of Forest Genetics and Plant Physiology, Swedish University of Agricultural Sciences, SE-901 83 Umea, Sweden
lib entry date25 January 2005
metabolite roleMST
retention time (sec)296.3
retention index (VAR5 method, n-alkanes C10–C36)1,665.24 (predicted, according to Strehmel, N. et.al)
base peak (m/z)73
maximal intensity999
mass-intensity-peaks cardinality185 intensities
minimal m/z54
maximal m/z469
download JCAMP DXSpectrumJcampDx.ashx?id=800c7418-1d8f-4bf7-95a3-4141aac6af0b
download MSPSpectrumMsp.ashx?id=800c7418-1d8f-4bf7-95a3-4141aac6af0b

GC-Method

nameM[MOR]
citationGullberg J, Jonsson P, Nordström A, Sjöström M, Moritz T (2004) Anal Biochem 331, 283-295
attributetextdetails
deconvolutionChromaTOF V1.00 (Pegasus Driver 1.61), LECO, St. Joseph, MI, USAOFFSET:NA; SMOOTHING:NA; WIDTH:2; SN:>10
derivatizationMEOX; TMSMETHOXYAMINATION: 60min60°C, 960min20°C; SILYLATION:>60min40°C
detectorMS-TOFm/z:50-800; SCANS:30/s; Pegasus III TOF-MS; LECO, St. Joseph, MI, USA
extractionmethanol:chloroform:water (3:1:1; v/v/v) 15min at 60°C 
ion sourceEI70eV
metabolic inactivationcut; liquid nitrogen; -80°C 
partitioningnone 
RIALKANEC12, C13, C14, C15, C16, C17, C18, C19, C20, C21, C22, C23, C24, C25
separationGCCOLUMN:5%diphenyl-95%dimethylpolysiloxane, 10m, ID:0.18mm, DF:0.18µm, DB-5-MS (J&W Scientific, Folsom, CA, USA); PROGRAM: iso 2min at 70°C, ramp 40°C/min, iso 1min at 320°C; FLOW:Helium, 1.0ml/min: INJECTION:1µL, splitless, 270°C; TRANSFER:250°C; IONSOURCE:200°C

comments on this mass spectrum

Post a Comment
Name:
 
Website:
Email:
Comments:
service last updated 31/08/2021 © 2008-2014 Golm Metabolome Database - All rights reserved
Top