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Lyxose (1MEOX) (4TMS) BP

 

Replica Mass Spectra of Lyxose (1MEOX) (4TMS) BP

replicalib entry datedetectionmethodspecies
1405 June 2013  MRI_2013 
1030 March 2011  Fiehn_GC_2010 
1130 March 2011  Fiehn_GC_2010 
325 January 2005 MS-TOFM[MOR] 
422 February 2005 MS-TOFM[STR] 
526 November 2004  M[FAME4090]Standard
1328 August 2012  MassBank GC 2010 Tsujimoto 
619 January 2005 MS-QUADM[ROE] 
1230 March 2011  Fiehn_GC_2010 
722 February 2005 MS-TOFM[STR] 
12 spectrum(a)
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Spectrum Details

analyteLyxose (1MEOX) (4TMS) BP
analyte InChIInChI=1S/C18H45NO5Si4/c1-20-19-14-16(22-26(5,6)7)18(24-28(11,12)13)17(23-27(8,9)10)15-21-25(2,3)4/h14,16-18H,15H2,1-13H3/b19-14-
analyte mass467.9
chromatogram6046hf_53
citation 
authorsBoelling C, Liebig F, Erban A, Kopka J, Max Planck Institute of Molecular Plant Physiology, Department of Molecular Plant Physiology (Prof. Willmitzer L), Am Muehlenberg 1, D-14476 Golm, Germany
lib entry date19 July 2007
metabolite roleMETB
retention time (sec)475.43
retention index (VAR5 method, n-alkanes C10–C36) 
base peak (m/z)73
maximal intensity1.083.053
mass-intensity-peaks cardinality435 intensities
minimal m/z45
maximal m/z1.000
download JCAMP DXSpectrumJcampDx.ashx?id=8df92b9e-616c-4008-ba2d-2239b67361e1
download MSPSpectrumMsp.ashx?id=8df92b9e-616c-4008-ba2d-2239b67361e1

GC-Method

nameMDN35
citationKopka J, Max Planck Institute of Molecular Plant Physiology, Department of Molecular Plant Physiology (Prof. Willmitzer L), Am Muehlenberg 1, D-14476 Golm, Germany
attributetextdetails
deconvolutionChromaTOFBASELINE OFFSET: 1; SMOOTHING: 5; PEAK WIDTH: 3s; S/N: 10
derivatizationMEOX; MSTFAMETHOXYAMINATION: 120min at 37°C; TRIMETHYLSILYLATION: 30min at 37°C
detectorMS-TOFm/z = 70-600; scans:20/s;
extractionchloroform:dH2O (2:1; v/v); chloroform (20°C); dH2O (4°C)
ion sourceEI70eV
RIFAME, d6-CholesteroleFAME: C8, C9, C10, C12, C14, C16, C18, C20, C22, C24, C26, C28, C30
separationGCCOLUMN:35%phenyl-65%dimethylpolysiloxane, 30m, ID:0.32mm, DF:0.25µm, MDN-35 (Macherey-Nagel, Düren, Germany); PROGRAM:iso 2min 80°C, ramp 15°C/min, iso 6min 330°C; FLOW:Helium, 2mL/min; INJECTION:1µL, splitless, 230°C; TRANSFER:250°C; IONSOURCE:250°C

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