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Salicylaldehyde-beta-D-glucopyranoside (1MEOX) (4TMS) BP (Derivate not found)

 

Replica Mass Spectra of Salicylaldehyde-beta-D-glucopyranoside (1MEOX) (4TMS) BP (Derivate not found)

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Spectrum Details

analyteSalicylaldehyde-beta-D-glucopyranoside (1MEOX) (4TMS) BP (Derivate not found)
analyte InChI
analyte mass602.03
chromatogram4029BB17
citation 
authorsKopka J, Max Planck Institute of Molecular Plant Physiology, Department of Molecular Plant Physiology (Prof. Willmitzer L), Am Muehlenberg 1, D-14476 Golm, Germany
lib entry date07 September 2004
metabolite roleMETB
retention time (sec)2,216.4
retention index (VAR5 method, n-alkanes C10–C36)2,564.72 (predicted, according to Strehmel, N. et.al)
base peak (m/z)73
maximal intensity999
mass-intensity-peaks cardinality229 intensities
minimal m/z41
maximal m/z496
download JCAMP DXSpectrumJcampDx.ashx?id=96d85c03-67d9-46ba-a2e2-5703a68001ff
download MSPSpectrumMsp.ashx?id=96d85c03-67d9-46ba-a2e2-5703a68001ff

GC-Method

nameM[2]
citationRoessner U, Wagner C, Kopka J, Trethewey RN, Willmitzer L (2000) Plant J 23, 131-142
attributetextdetails
deconvolutionAMDIS, National Institute of Standards and Technology, Gaithersburg, MD, USADIRECTION:Low to High; WIDTH: 20; SUBTRACTION: two; RESOLUTION: low; SENSITIVITY: low; SHAPE: low
derivatizationMEOX; TMSMethoxyamination:60min37°C; Trimethylsilylation:>45min37°C
detectorMS-Quadm/z = 35-600; scans:2/s; MD 800 Thermo-Finnigan, San Jose, CA, USA
extractionmethanol:water (4:1; v/v); 15min70°C 
ion sourceEI70eV
metabolic inactivationcut; liquid nitrogen; -80°C 
partitioningmethanol fraction of a methanol:water:chloroform (approx. 2:2:1, v/v/v) partitioning 
RIALKANEC12, C15, C19, C22, C28, C32, C36
separationGCCOLUMN:5%diphenyl-95%dimethylpolysiloxane (arylene), 30+10m, ID:0.25mm, DF:0.25microm, Rtx-5SilMS Integra-Guard, #NA (Restek, Bad Homburg, Germany); PROGRAM:iso1min70°C, ramp9°C/min, iso5min350°C; FLOW:Helium, 0.6ml/min; INJECTION:1microL, splitless, 230°C; TRANSFER:250°C; IONSOURCE:250°C

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