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Lysine (3TMS)

 

Replica Mass Spectra of Lysine (3TMS)

replicalib entry datedetectionmethodspecies
101 May 2001 MS-TOFM[EIGTMS]Standard Addition
201 November 2001 MS-TOFM[EIGTMS]Corynebacterium glutamicum
1430 March 2011  Fiehn_GC_2010 
412 October 2005 MS-TRAPM[BAR] 
519 July 2007 MS-TOFVAR5Reference Substance
619 July 2007 MS-TOFVAR5Reference Substance
719 July 2007 MS-TOFVAR5Reference Substance
1528 August 2012  MassBank GC 2010 Ara 
801 December 2003 MS-QuadM[2]Standard
1303 November 2010  Schomburg_GC_2010 
15 spectrum(a)
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Spectrum Details

analyteLysine (3TMS)
analyte InChI
analyte mass362.73
chromatogram4132GX21
citation 
authorsLiebig F, Erban A, Max Planck Institute of Molecular Plant Physiology, Department of Molecular Plant Physiology (Prof. Willmitzer L), Am Muehlenberg 1, D-14476 Golm, Germany
lib entry date15 March 2005
metabolite roleMETB
retention time (sec)1,169.29
retention index (VAR5 method, n-alkanes C10–C36)1.848,63 (predicted, according to Strehmel, N. et.al)
base peak (m/z)73
maximal intensity999
mass-intensity-peaks cardinality72 intensities
minimal m/z70
maximal m/z363
download JCAMP DXSpectrumJcampDx.ashx?id=9b4c8ac3-16d9-4915-a01a-340f91146fc0
download MSPSpectrumMsp.ashx?id=9b4c8ac3-16d9-4915-a01a-340f91146fc0

GC-Method

nameM[6]
citationErban A, Schauer N, Fernie AR, Kopka J (2006) In: Weckwerth W (ed): Methods in Molecular Biology Vol., Humana Press Inc., Totowa, USA
attributetextdetails
deconvolutionChromaTOF V1.00 (Pegasus Driver 1.61), LECO, St. Joseph, MI, USAOFFSET:1_SMOOTHING:3_WIDTH:6_SN:>2
derivatizationMEOX; TMSMethoxyamination:90min40°C; Trimethylsilylation:45min40°C
detectorMS-TOFMZ:70-600; SCANS:20/s; Pegasus III TOF-MS; LECO, St. Joseph, MI, USA
extractionmethanol:water (4:1; v/v); 15min70°C 
ion sourceEI70eV
metabolic inactivationcut; liquid nitrogen; -80°C 
partitioningmethanol fraction of a methanol:water:chloroform (approx. 2:2:1, v/v/v) partitioning 
RIALKANEC12, C15, C18, C19, C22, C28, C32, C36
separationGCCOLUMN:5%diphenyl-95%dimethylpolysiloxane (arylene), 30+10m, ID:0.25mm, DF:0.25microm, Rtx-5SilMS Integra-Guard, #525560 (Restek, Bad Homburg, Germany); PROGRAM:iso1min70°C, ramp9°C/min, iso5min350°C; FLOW:Helium, 0.6ml/min; INJECTION:1microL, splitless, 230°C; TRANSFER:250°C; IONSOURCE:250°C

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