GOLM METABOLOME DATABASE
How would you rate the quality of this mass spectrum?
poor, not helpful 
 outstanding, most helpful.
This spectrum was 0 times rated; on average=0.0

Lactic acid, 3-phenyl- (2TMS)

 

Replica Mass Spectra of Lactic acid, 3-phenyl- (2TMS)

replicalib entry datedetectionmethodspecies
528 August 2012  MassBank GC 2010 Tsujimoto 
605 June 2013  MRI_2013 
219 July 2007 MS-TOFVAR5Reference Substance
330 March 2011  Fiehn_GC_2010 
430 March 2011  Fiehn_GC_2010 
5 spectrum(a)
rotate: click+drag; translate: alt+click+drag; zoom: mousewheel; save: mol

Spectrum Details

analyteLactic acid, 3-phenyl- (2TMS)
analyte InChIInChI=1S/C15H26O3Si2/c1-19(2,3)17-14(15(16)18-20(4,5)6)12-13-10-8-7-9-11-13/h7-11,14H,12H2,1-6H3/t14-/m0/s1
analyte mass310.54
chromatogram6030hf_14
citation 
authorsBoelling C, Liebig F, Erban A, Kopka J, Max Planck Institute of Molecular Plant Physiology, Department of Molecular Plant Physiology (Prof. Willmitzer L), Am Muehlenberg 1, D-14476 Golm, Germany
lib entry date19 July 2007
metabolite role 
retention time (sec)500.71
retention index (VAR5 method, n-alkanes C10–C36) 
base peak (m/z)73
maximal intensity1,730,350
mass-intensity-peaks cardinality498 intensities
minimal m/z45
maximal m/z1,000
download JCAMP DXSpectrumJcampDx.ashx?id=d01e822b-957a-476e-b814-525538f8138f
download MSPSpectrumMsp.ashx?id=d01e822b-957a-476e-b814-525538f8138f

GC-Method

nameMDN35
citationKopka J, Max Planck Institute of Molecular Plant Physiology, Department of Molecular Plant Physiology (Prof. Willmitzer L), Am Muehlenberg 1, D-14476 Golm, Germany
attributetextdetails
deconvolutionChromaTOFBASELINE OFFSET: 1; SMOOTHING: 5; PEAK WIDTH: 3s; S/N: 10
derivatizationMEOX; MSTFAMETHOXYAMINATION: 120min at 37°C; TRIMETHYLSILYLATION: 30min at 37°C
detectorMS-TOFm/z = 70-600; scans:20/s;
extractionchloroform:dH2O (2:1; v/v); chloroform (20°C); dH2O (4°C)
ion sourceEI70eV
RIFAME, d6-CholesteroleFAME: C8, C9, C10, C12, C14, C16, C18, C20, C22, C24, C26, C28, C30
separationGCCOLUMN:35%phenyl-65%dimethylpolysiloxane, 30m, ID:0.32mm, DF:0.25µm, MDN-35 (Macherey-Nagel, Düren, Germany); PROGRAM:iso 2min 80°C, ramp 15°C/min, iso 6min 330°C; FLOW:Helium, 2mL/min; INJECTION:1µL, splitless, 230°C; TRANSFER:250°C; IONSOURCE:250°C

comments on this mass spectrum

Post a Comment
Name:
 
Website:  
Email:
Comments:
service last updated 31/08/2021 © 2008-2014 Golm Metabolome Database - All rights reserved
Top