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Xylose (1MEOX) (4TMS) BP

 

Replica Mass Spectra of Xylose (1MEOX) (4TMS) BP

replicalib entry datedetectionmethodspecies
122 February 2005 MS-TOFM[STR] 
2728 August 2012  MassBank GC 2010 Tsujimoto 
222 February 2005 MS-TOFM[STR] 
301 August 2002 MS-QuadM[2]Lotus japonicus (Regel) K. Larsen
2523 July 2012 MS-TOFVAR5 
401 August 2002 MS-QuadM[2]Lotus japonicus (Regel) K. Larsen
2805 June 2013  MRI_2013 
501 August 2002 MS-QuadM[2]Lotus japonicus (Regel) K. Larsen
601 May 2001 MS-TOFM[EIGTMS]Solanum tuberosum
701 February 2005 MS-TOFM[6]Reference Substance
26 spectrum(a)
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Spectrum Details

analyteXylose (1MEOX) (4TMS) BP
analyte InChIInChI=1S/C18H45NO5Si4/c1-20-19-14-16(22-26(5,6)7)18(24-28(11,12)13)17(23-27(8,9)10)15-21-25(2,3)4/h14,16-18H,15H2,1-13H3/b19-14-/t16-,17+,18+/m0/s1
analyte mass467.9
chromatogramNA(_43)
citation 
authorsMoritz T, Umea Plant Science Centre, Department of Forest Genetics and Plant Physiology, Swedish University of Agricultural Sciences, SE-901 83 Umea, Sweden
lib entry date25 January 2005
metabolite roleMETB
retention time (sec)294.2
retention index (VAR5 method, n-alkanes C10–C36)1,652.85 (predicted, according to Strehmel, N. et.al)
base peak (m/z)73
maximal intensity999
mass-intensity-peaks cardinality157 intensities
minimal m/z53
maximal m/z467
download JCAMP DXSpectrumJcampDx.ashx?id=d46e1acf-7696-4b9a-9c03-5eecd8384bbf
download MSPSpectrumMsp.ashx?id=d46e1acf-7696-4b9a-9c03-5eecd8384bbf

GC-Method

nameM[MOR]
citationGullberg J, Jonsson P, Nordström A, Sjöström M, Moritz T (2004) Anal Biochem 331, 283-295
attributetextdetails
deconvolutionChromaTOF V1.00 (Pegasus Driver 1.61), LECO, St. Joseph, MI, USAOFFSET:NA; SMOOTHING:NA; WIDTH:2; SN:>10
derivatizationMEOX; TMSMETHOXYAMINATION: 60min60°C, 960min20°C; SILYLATION:>60min40°C
detectorMS-TOFm/z:50-800; SCANS:30/s; Pegasus III TOF-MS; LECO, St. Joseph, MI, USA
extractionmethanol:chloroform:water (3:1:1; v/v/v) 15min at 60°C 
ion sourceEI70eV
metabolic inactivationcut; liquid nitrogen; -80°C 
partitioningnone 
RIALKANEC12, C13, C14, C15, C16, C17, C18, C19, C20, C21, C22, C23, C24, C25
separationGCCOLUMN:5%diphenyl-95%dimethylpolysiloxane, 10m, ID:0.18mm, DF:0.18µm, DB-5-MS (J&W Scientific, Folsom, CA, USA); PROGRAM: iso 2min at 70°C, ramp 40°C/min, iso 1min at 320°C; FLOW:Helium, 1.0ml/min: INJECTION:1µL, splitless, 270°C; TRANSFER:250°C; IONSOURCE:200°C

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