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Spermine (6TMS)

 

Replica Mass Spectra of Spermine (6TMS)

replicalib entry datedetectionmethodspecies
119 July 2007 MS-TOFVAR5Reference Substance
1528 August 2012  MassBank GC 2010 Ara 
215 March 2005 MS-TOFM[6]Reference Substance
315 March 2005 MS-TOFM[6]Reference Substance
401 February 2005 MS-TOFM[6]Reference Substance
1428 August 2012  MassBank GC 2010 Tsujimoto 
619 July 2007 MS-TOFVAR5Reference Substance
726 November 2004  M[FAME4090]Standard
815 March 2005 MS-TOFM[6]Reference Substance
901 April 2002 MS-QuadM[2]Standard
14 spectrum(a)
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Spectrum Details

analyteSpermine (6TMS)
analyte InChIInChI=1S/C28H74N4Si6/c1-33(2,3)29(25-21-27-31(35(7,8)9)36(10,11)12)23-19-20-24-30(34(4,5)6)26-22-28-32(37(13,14)15)38(16,17)18/h19-28H2,1-18H3
analyte mass635.43
chromatogram6058hf_51
citation 
authorsBoelling C, Liebig F, Erban A, Kopka J, Max Planck Institute of Molecular Plant Physiology, Department of Molecular Plant Physiology (Prof. Willmitzer L), Am Muehlenberg 1, D-14476 Golm, Germany
lib entry date19 July 2007
metabolite roleMETB
retention time (sec)864.63
retention index (VAR5 method, n-alkanes C10–C36) 
base peak (m/z)116
maximal intensity127,354
mass-intensity-peaks cardinality603 intensities
minimal m/z45
maximal m/z1,000
download JCAMP DXSpectrumJcampDx.ashx?id=d6771a38-75c6-4074-b7c8-925c934c9d98
download MSPSpectrumMsp.ashx?id=d6771a38-75c6-4074-b7c8-925c934c9d98

GC-Method

nameMDN35
citationKopka J, Max Planck Institute of Molecular Plant Physiology, Department of Molecular Plant Physiology (Prof. Willmitzer L), Am Muehlenberg 1, D-14476 Golm, Germany
attributetextdetails
deconvolutionChromaTOFBASELINE OFFSET: 1; SMOOTHING: 5; PEAK WIDTH: 3s; S/N: 10
derivatizationMEOX; MSTFAMETHOXYAMINATION: 120min at 37°C; TRIMETHYLSILYLATION: 30min at 37°C
detectorMS-TOFm/z = 70-600; scans:20/s;
extractionchloroform:dH2O (2:1; v/v); chloroform (20°C); dH2O (4°C)
ion sourceEI70eV
RIFAME, d6-CholesteroleFAME: C8, C9, C10, C12, C14, C16, C18, C20, C22, C24, C26, C28, C30
separationGCCOLUMN:35%phenyl-65%dimethylpolysiloxane, 30m, ID:0.32mm, DF:0.25µm, MDN-35 (Macherey-Nagel, Düren, Germany); PROGRAM:iso 2min 80°C, ramp 15°C/min, iso 6min 330°C; FLOW:Helium, 2mL/min; INJECTION:1µL, splitless, 230°C; TRANSFER:250°C; IONSOURCE:250°C

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