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Glucose, 2-deoxy- (1MEOX) (4TMS) MP

 

Replica Mass Spectra of Glucose, 2-deoxy- (1MEOX) (4TMS) MP

replicalib entry datedetectionmethodspecies
1305 June 2013  MRI_2013 
1103 November 2010  Schomburg_GC_2010 
219 July 2007 MS-TOFVAR5Reference Substance
808 December 2010 MS-TOFVAR5 
1228 August 2012  MassBank GC 2010 Tsujimoto 
322 January 2005 MS-QUADM[ROE] 
908 December 2010 MS-TOFVAR5 
1008 December 2010 MS-TOFVAR5 
426 November 2004  M[FAME4090]Standard
522 February 2005 MS-TOFM[STR] 
12 spectrum(a)
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Spectrum Details

analyteGlucose, 2-deoxy- (1MEOX) (4TMS) MP
analyte InChIInChI=1S/C19H47NO5Si4/c1-21-20-15-14-17(23-27(5,6)7)19(25-29(11,12)13)18(24-28(8,9)10)16-22-26(2,3)4/h15,17-19H,14,16H2,1-13H3/b20-15+/t17-,18-,19+/m1/s1
analyte mass481.92
chromatogram6044hf_6
citation 
authorsBoelling C, Liebig F, Erban A, Kopka J, Max Planck Institute of Molecular Plant Physiology, Department of Molecular Plant Physiology (Prof. Willmitzer L), Am Muehlenberg 1, D-14476 Golm, Germany
lib entry date19 July 2007
metabolite roleMETB
retention time (sec)545.43
retention index (VAR5 method, n-alkanes C10–C36) 
base peak (m/z)73
maximal intensity1.435.839
mass-intensity-peaks cardinality374 intensities
minimal m/z45
maximal m/z1.000
download JCAMP DXSpectrumJcampDx.ashx?id=f2569a2a-4e59-4ae6-96fd-2030c85315fc
download MSPSpectrumMsp.ashx?id=f2569a2a-4e59-4ae6-96fd-2030c85315fc

GC-Method

nameMDN35
citationKopka J, Max Planck Institute of Molecular Plant Physiology, Department of Molecular Plant Physiology (Prof. Willmitzer L), Am Muehlenberg 1, D-14476 Golm, Germany
attributetextdetails
deconvolutionChromaTOFBASELINE OFFSET: 1; SMOOTHING: 5; PEAK WIDTH: 3s; S/N: 10
derivatizationMEOX; MSTFAMETHOXYAMINATION: 120min at 37°C; TRIMETHYLSILYLATION: 30min at 37°C
detectorMS-TOFm/z = 70-600; scans:20/s;
extractionchloroform:dH2O (2:1; v/v); chloroform (20°C); dH2O (4°C)
ion sourceEI70eV
RIFAME, d6-CholesteroleFAME: C8, C9, C10, C12, C14, C16, C18, C20, C22, C24, C26, C28, C30
separationGCCOLUMN:35%phenyl-65%dimethylpolysiloxane, 30m, ID:0.32mm, DF:0.25µm, MDN-35 (Macherey-Nagel, Düren, Germany); PROGRAM:iso 2min 80°C, ramp 15°C/min, iso 6min 330°C; FLOW:Helium, 2mL/min; INJECTION:1µL, splitless, 230°C; TRANSFER:250°C; IONSOURCE:250°C

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