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Tyramine (3TMS)

 

Replica Mass Spectra of Tyramine (3TMS)

replicalib entry datedetectionmethodspecies
111 September 2005  M[FAME4090]Standard
1528 August 2012  MassBank GC 2010 Kusano 
1805 June 2013  MRI_2013 
1430 March 2011  Fiehn_GC_2010 
301 May 2001 MS-TOFM[EIGTMS]Nicotiana tabacum
426 November 2004  M[FAME4090]Standard
525 January 2005 MS-TOFM[MOR] 
619 January 2005 MS-QUADM[ROE] 
701 September 2001 MS-QuadM[2]Standard Addition
911 September 2005  M[FAME4090]Standard
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Spectrum Details

analyteTyramine (3TMS)
analyte InChIInChI=1S/C17H35NOSi3/c1-20(2,3)18(21(4,5)6)15-14-16-10-12-17(13-11-16)19-22(7,8)9/h10-13H,14-15H2,1-9H3
analyte mass353.72
chromatogram2011EC35
citationWagner C, Sefkow M, Kopka J (2003) Phytochemistry 62, 887-900
authorsKopka J, Max Planck Institute of Molecular Plant Physiology, Department of Molecular Plant Physiology (Prof. Willmitzer L), Am Muehlenberg 1, D-14476 Golm, Germany
lib entry date01 January 2002
metabolite roleMETB
retention time (sec) 
retention index (VAR5 method, n-alkanes C10–C36)1,912 (predicted, according to Strehmel, N. et.al)
base peak (m/z)174
maximal intensity999
mass-intensity-peaks cardinality144 intensities
minimal m/z70
maximal m/z352
download JCAMP DXSpectrumJcampDx.ashx?id=febf9636-6d2b-48a9-8321-17741ce1b639
download MSPSpectrumMsp.ashx?id=febf9636-6d2b-48a9-8321-17741ce1b639

GC-Method

nameM[EIGTMS]
citationWagner C, Sefkow M, Kopka J (2003) Phytochemistry 62, 887-900
attributetextdetails
deconvolutionAMDIS, National Institute of Standards and Technology, Gaithersburg, MD, USADIRECTION:non scanning; WIDTH: 20; SUBTRACTION: two; RESOLUTION: high; SENSITIVITY: medium; SHAPE: high
derivatizationMEOX; TMSMethoxyamination:60min37°C; Trimethylsilylation:>60min37°C
detectorMS-TOFMZ:70-600; SCANS:6/s; Pegasus II TOF-MS; LECO, St. Joseph, MI, USA
extractionmethanol:water (4:1; v/v); 15min70°C 
ion sourceEI70eV
metabolic inactivationcut; liquid nitrogen; -80°C 
partitioningmethanol fraction of a methanol:water:chloroform (approx. 2:2:1, v/v/v) partitioning 
RIALKANEC12, C15, C19, C22, C28, C32, C36
separationGCCOLUMN:5%diphenyl-95%dimethylpolysiloxane (arylene), 30+10m, ID:0.25mm, DF:0.25microm, Rtx-5SilMS Integra-Guard, #NA (Restek, Bad Homburg, Germany); PROGRAM:iso2min80°C, ramp15°C/min, iso2min350°C; FLOW:Helium, 1.0ml/min; INJECTION:1microL, splitless, 230°C, 2min110psi; TRANSFER:250°C; IONSOURCE:200°C

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