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Octadecane, n-

 

Replica Mass Spectra of Octadecane, n-

replicalib entry datedetectionmethodspecies
627 June 2008 MS-TOFVAR5na
523 June 2008 MS-TOFVAR5na
727 June 2008 MS-TOFVAR5na
1123 July 2012 MS-TOFVAR5 
112 May 2005  M[NIST] 
827 June 2008 MS-TOFVAR5na
927 June 2008 MS-TOFVAR5na
301 May 2003 MS-QuadM[2]Spathodea campanulata P. Beauv.
401 December 2003 MS-QuadM[2]Standard Addition
1003 February 2011 MS-TOFVAR5 
10 spectrum(a)
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Spectrum Details

analyteOctadecane, n-
analyte InChIInChI=1S/C18H38/c1-3-5-7-9-11-13-15-17-18-16-14-12-10-8-6-4-2/h3-18H2,1-2H3
analyte mass254.49
chromatogramNA(_58)
citation 
authorsMoritz T, Umea Plant Science Centre, Department of Forest Genetics and Plant Physiology, Swedish University of Agricultural Sciences, SE-901 83 Umea, Sweden
lib entry date25 January 2005
metabolite roleIS (RI05)
retention time (sec)319.6
retention index (VAR5 method, n-alkanes C10–C36)1,801.48 (predicted, according to Strehmel, N. et.al)
base peak (m/z)57
maximal intensity999
mass-intensity-peaks cardinality50 intensities
minimal m/z53
maximal m/z255
download JCAMP DXSpectrumJcampDx.ashx?id=162cd4e1-355b-40d1-a531-55dc1dd35598
download MSPSpectrumMsp.ashx?id=162cd4e1-355b-40d1-a531-55dc1dd35598

GC-Method

nameM[MOR]
citationGullberg J, Jonsson P, Nordström A, Sjöström M, Moritz T (2004) Anal Biochem 331, 283-295
attributetextdetails
deconvolutionChromaTOF V1.00 (Pegasus Driver 1.61), LECO, St. Joseph, MI, USAOFFSET:NA; SMOOTHING:NA; WIDTH:2; SN:>10
derivatizationMEOX; TMSMETHOXYAMINATION: 60min60°C, 960min20°C; SILYLATION:>60min40°C
detectorMS-TOFm/z:50-800; SCANS:30/s; Pegasus III TOF-MS; LECO, St. Joseph, MI, USA
extractionmethanol:chloroform:water (3:1:1; v/v/v) 15min at 60°C 
ion sourceEI70eV
metabolic inactivationcut; liquid nitrogen; -80°C 
partitioningnone 
RIALKANEC12, C13, C14, C15, C16, C17, C18, C19, C20, C21, C22, C23, C24, C25
separationGCCOLUMN:5%diphenyl-95%dimethylpolysiloxane, 10m, ID:0.18mm, DF:0.18µm, DB-5-MS (J&W Scientific, Folsom, CA, USA); PROGRAM: iso 2min at 70°C, ramp 40°C/min, iso 1min at 320°C; FLOW:Helium, 1.0ml/min: INJECTION:1µL, splitless, 270°C; TRANSFER:250°C; IONSOURCE:200°C

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