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Replica Mass Spectra of Spermine (5TMS) MP
replica | lib entry date | detection | method | species |
1 | 19 July 2007 | MS-TOF | MDN35 | Reference Substance |
2 | 19 July 2007 | MS-TOF | VAR5 | Reference Substance |
3 | 15 March 2005 | MS-TOF | M[6] | Reference Substance |
4 | 19 July 2007 | MS-TOF | MDN35 | Reference Substance |
5 | 01 April 2002 | MS-Quad | M[2] | Standard |
7 | 15 March 2005 | MS-TOF | M[6] | Reference Substance |
14 | 28 August 2012 | | MassBank GC 2010 Kusano | |
8 | 26 November 2004 | | M[FAME4090] | Standard |
9 | 15 March 2005 | MS-TOF | M[6] | Reference Substance |
10 | 19 July 2007 | MS-TOF | VAR5 | Reference Substance |
13 spectrum(a) |
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Spectrum Details
GC-Method
name | M[ROE] |
citation | U. Roessner, J. Patterson, M. Forbes, G. Fincher, P. Langridge, A. Bacic, Plant Physiology 142 (2006) 1087 |
attribute | text | details |
deconvolution | Xcalibur program | |
derivatization | MEOX; MSTFA | METHOXYAMINATION: 120min at 37°C; SILYLATION: 30min at 37°C |
detector | MS-QUAD | m/z = 70-600; scans:2/s; DSQ quadrupole mass spectrometer |
extraction | methanol:chloroform | |
ion source | EI | 70eV |
RI | ALKANE | C12, C15, C19, C22, C28, C32, C36 |
separation | GC | COLUMN:5%diphenyl-95%dimethylpolysiloxane, 30+10m, ID:0.25mm, DF:0.25µm, VF-5MS (Varian, Darmstadt, Germany); PROGRAM:injection at 70°C, ramp 1°C/min to 76°C, ramp 6°C/min to 330°C, iso at 330°C for 10min; FLOW:Helium, 1mL/min; INJECTION:1µL, splitless, 230°C; TRANSFER:280°C; IONSOURCE:250°C |
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